Mahadevan, C. ; Seshasayee, M. ; Ramakrishna, B. L. ; Manoharan, P. T. (1985) Structure of dichlorobis[P,P,P',P'-tetramethyl-o-phenylenebis(phosphine)]nickel(III) hexafluorophosphate dihydrate, [NiCl2{P2(CH3)4(C6H4)}2]PF6.2H2O Acta Crystallographica Section C, 41 (1). pp. 38-40. ISSN 0108-2701
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Official URL: http://scripts.iucr.org/cgi-bin/paper?S01082701850...
Related URL: http://dx.doi.org/10.1107/S0108270185002700
Abstract
Mr=706.9, monoclinic, C2/m, a=12.467(6), b=10.497), c=11.241(7)Å, β=100.79(4), V=1445 Å3, Z=2, Dx=1.625 Mg m-3, Mo Ka, λ=0.71069 Å, μ=1.108 mm-1, F(000)=726, room temperature, final R=0.087 for 1365 unique reflections. The Ni atom has a tetragonally distorted octahedral configuration with chlorine atoms in the axial positions and the anionic P atom has a regular are 2.424(4) and 2.255(3) Å. The anion and cation are held together by van der Waals forces.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to International Union of Crystallography. |
| ID Code: | 95690 |
| Deposited On: | 20 Nov 2012 10:57 |
| Last Modified: | 20 Nov 2012 10:57 |
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