Tensile properties of modified 9Cr-1Mo steel by shear punch testing and correlation with microstructures

Abstract

Modified 9Cr-1Mo ferritic steel (P91) is subjected to a series of heat treatments consisting of soaking for 5 min at the selected temperatures in the range 973 K-162₃ K (below Ac₁ to above Ac₄) followed by oil quenching and tempering at 1033 K for 1 h to obtain different microstructural conditions. The tensile properties of the different microstructural conditions are evaluated from small volumes of material by shear punch test technique. A new methodology for evaluating yield strength, ultimate tensile strength and strain hardening exponent from shear punch test by using correlation equations without employing empirical constants is presented and validated. The changes in the tensile properties are related to the microstructural changes of the steel investigated by electron microscopic studies. The steel exhibits minimum strength and hardness when soaked between Ac₁ and Ac₃ (intercritical range) temperatures due to the replacement of original lath martensitic structure with subgrains. The finer martensitic microstructure produced in the steel after soaking at temperatures above Ac₃ leads to a monotonic increase in hardness and strength with decreasing strain hardening exponent. For soaking temperatures above Ac₄, the hardness and strength of the steel increases marginally due to the formation of soft δ ferrite.