Microwave-assisted preparation and sintering of mullite and mullite-zirconia composites from metalorganics

Ravi, B. G. ; Praveen, V. ; Panneer Selvam, M. ; Rao, K. J. (1998) Microwave-assisted preparation and sintering of mullite and mullite-zirconia composites from metalorganics Materials Research Bulletin, 33 (10). pp. 1527-1536. ISSN 0025-5408

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Official URL: http://www.sciencedirect.com/science/article/pii/S...

Related URL: http://dx.doi.org/10.1016/S0025-5408(98)00135-4

Abstract

Decomposition characteristics of a mixture of aluminum-tri-sec butoxide (ASB) and tetraethyl orthosilicate (TEOS) in ethyl acetate solution by microwave pyrolysis was examined. The decomposed product was used as a second-stage precursor in the preparation of pure mullite (3Al2O3.2SiO2). Mullite-zirconia composites were obtained, using the aLtd mixture along with zirconium-iso-propoxide as starting materials. Pellets of mullite and mullite-zirconia composites were sintered in a microwave oven using β -SiC as a secondary heater.

Item Type:Article
Source:Copyright of this article belongs to Elsevier Science.
Keywords:A. ceramics; A. composites; C. thermogravimetric analysis (TGA); C. X-ray diffraction; D. microstructure
ID Code:91126
Deposited On:17 May 2012 04:24
Last Modified:17 May 2012 04:24

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