Mathur, Pradeep ; Manimaran, Bala ; Trivedi, Rajiv ; Munkir Hossain, Md. ; Arabatti, Mangla (1996) Synthesis, spectroscopic and structural characterisation of {(CO)3Fe(μ-CH2)Se}2 and (CO)6Fe2}μ-Se(CH2)nSe}(n = 1, 2) Journal of Organometallic Chemistry, 515 (1-2). pp. 155-162. ISSN 0022-328X
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Official URL: http://www.sciencedirect.com/science/article/pii/0...
Related URL: http://dx.doi.org/10.1016/0022-328X(95)06056-3
Abstract
From the room temperature reaction of (CO)9Fe3(μ3-Se)2 or (CO)6Fe2(μ-Se2) with diazomethane, four products were isolated; {(CO)3Fe(μ-CH2)Se}2 (1), (CO)6Fe2(μ-SeCH3)2 (2), (CO)6Fe2(μ-SeCH2Se) (3) and (CO)6Fe2(μ-SeCH2CH2Se) (4). All four compounds were characterised by IR, 1H, 13C, and 77Se NMR spectroscopy. Structures of 1, 3 and 4 were established by single crystal X-ray structure analyses.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Elsevier Science. |
| Keywords: | Iron; Selenium; Methylene; Carbonyl; X-ray Diffraction; Crystal Structure |
| ID Code: | 83056 |
| Deposited On: | 16 Feb 2012 07:50 |
| Last Modified: | 16 Feb 2012 07:50 |
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