Kedarnath, G. ; Dey, Sandip ; Jain, Vimal K. ; Dey, Gautam K. (2006) Synthesis and characterization of metal selenide (ZnSe, CdSe, HgSe) nanoparticles Journal of Nanoscience and Nanotechnology, 6 (4). pp. 1031-1037. ISSN 1533-4880
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Official URL: http://www.ingentaconnect.com/content/asp/jnn/2006...
Related URL: http://dx.doi.org/10.1166/jnn.2006.154
Abstract
Thermolysis of [M(SeCH2CH2CH2NMe2)2] (M = Zn, Cd, Hg), prepared by the reactions of sodium salt of 3-(N,N-dimethylamino)propaneselenolate with metal acetates, afforded metal selenides (MSe). The metal selenides were characterized by XRD, EDAX, SEM, AFM, and TEM techniques. Nanoparticles of HgSe were prepared by pyrolysis in a quartz boat, solvothermal, and sonochemical methods. EDAX showed 1:1 Hg/Se ratio, while XRD and SAED patterns confirmed the formation of cubic HgSe. These particles are spherical in nature with an average diameter of 15 nm (from TEM).
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to American Scientific Publishers. |
| Keywords: | ZNSE; CDSE; HGSE; Nanoparticles; N.N-dimethylaminopropaneselenolates |
| ID Code: | 82306 |
| Deposited On: | 10 Feb 2012 04:48 |
| Last Modified: | 10 Feb 2012 04:48 |
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