Acharya, K. R. ; Tavale, S. S. ; Guru Row, T. N. ; Venkatesan, K. (1984) Structure of 1-diphenylmethyl-3-hydroxyazetidinium chloride, C16H18NO+.Cl- Acta Crystallographica Section C, 40 (5). pp. 846-848. ISSN 0108-2701
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Official URL: http://scripts.iucr.org/cgi-bin/paper?S01082701840...
Related URL: http://dx.doi.org/10.1107/S0108270184005953
Abstract
Mr=275.8, monoclinic, P21/a, a=12.356 (5), b=9.054 (4), c= 14.043 (4) Å, β=100.34 (3) °, V=1545.5 Å3, Z=4, Dm=1.14, Dx = 1.185 Mg m-3, μ (Mo Kα, λ= 0.7107 Å ) 2.77 mm-1, F(000)=584.0, T=293 K, R=0.053 for 1088 reflections. The four-membered ring is buckled 13.0° (θ=167.0°). The azetidinium moiety is linked to the C1-ion through a hydrogen bond [O-H…C1=3.166 (5) Å].
| Item Type: | Article |
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| Source: | Copyright of this article belongs to International Union of Crystallography. |
| ID Code: | 66676 |
| Deposited On: | 27 Oct 2011 04:07 |
| Last Modified: | 11 Jul 2012 03:56 |
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