Ramakumar, S. ; Venkatesan, K. ; Rao, S. T. (1977) The crystal and molecular structure of 1-(diphenylmethyl)azetidin-3-ol Acta Crystallographica - Section B: Structural Crystallography & Crystal Chemistry, 33 (3). pp. 824-829. ISSN 0567-7408
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Official URL: http://scripts.iucr.org/cgi-bin/paper?S05677408770...
Related URL: http://dx.doi.org/10.1107/S0567740877004713
Abstract
1-(Diphenylmethyl)azetidin-3-ol is triclinic, space group P1, with a=8.479 (2), b=17.294 (4), c=10.606 (3) Å, α=118.59 (2), β=100.30 (2), γ=89.63 (2)°, Z=4. The structure was solved by multisolution methods and refined to an R of 0.044 for 2755 reflexions. The four-membered rings in the two independent molecules are puckered with dihedral angles of 156 and 153° . The two molecules differ in conformation with respect to rotation of the phenyl rings about the C-C bonds. The structure is stabilized by a network of O-H … N intermolecular hydrogen bonds.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to International Union of Crystallography. |
| ID Code: | 66661 |
| Deposited On: | 27 Oct 2011 04:03 |
| Last Modified: | 27 Oct 2011 04:03 |
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