High-temperature crack growth in monolithic and SiC_w-reinforced silicon nitride under static and cyclic loads

Abstract

Experimental results are presented on subcritical crack growth under sustained and cyclic loads in a HIPed Si₃N₄ at 1450° C and a hot-pressed Si₃N₄-10 vol% SiC_w composite in the temperature range 1300°-1400°C. Static and cyclic crack growth rates are obtained from the threshold for the onset of stable fracture with different cyclic frequencies and load ratios. Fatigue crack growth rates for both the monolithic and SiC_w-reinforced Si₃N₄ are generally higher than the crack growth velocities predicted using static crack growth data. However, the threshold stress intensity factor ranges for the onset of crack growth are always higher under cyclic loads than for sustained load fracture. Electron microscopy of crack wake contact and crack-tip damage illustrate the mechanisms of subcritical crack growth under static and cyclic loading. Critical experiments have been conducted systematically to measure the fracture initiation toughness at room temperature, after advancing the crack subcritically by a controlled amount under static or cyclic loads at elevated temperatures. Results of these experiments quantify the extent of degradation in crack-wake bridging due to cyclically varying loads. The effects of preexisting glass phase on elevated temperature fatigue and fracture are examined, and the creep crack growth behavior of Si₃N₄-based ceramics is compared with that of oxide-based ceramics.