Mandal, S. ; Bachman, R. E. ; Whitmire, K. H. ; Bharadwaj, P. K. (1992) Dichlorotetrakis(pyridine)nickel(II) Acta Crystallographica Section C: Crystal Structure Communications, 48 (10). pp. 1836-1837. ISSN 0108-2701
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Official URL: http://onlinelibrary.wiley.com/doi/10.1107/S010827...
Related URL: http://dx.doi.org/10.1107/S0108270192001872
Abstract
[NiCl2(C5H5N)4], Mr = 446.01, tetragonal, I4l/acd, a = 15.783 (3), c = 16.965 (8) Å, V = 4226 (2) Å3, Z=8, Dx = 1.402 Mg m-3, Mo Kα radiation (graphite-crystal monochromator). λ = 0.71069 Å, μ = 1, 19 mm-1, F(000) = 1840, T = 193 K, final conventional R = 0.039 for 741 unique observed [I > 3σ(I)] reflections and 83 variables. The Ni has an octahedral coordination with the CI ligands in a trans relationship. The Ni-CI distance is 2.433 (1) Å and the Ni-N distance is 2.121 (3) Å. The average N-Ni··CI angle is 90.0 (9)°.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to International Union of Crystallography. |
| ID Code: | 4941 |
| Deposited On: | 18 Oct 2010 06:13 |
| Last Modified: | 18 May 2011 09:30 |
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