Basavaiah, Deevi ; Reddy, Kanumuri Ramesh ; Kumaragurubaran, Nagaswamy (2007) An expedient, facile and simple one-pot synthesis of 2-methylenealkanoates and alkanenitriles from the Baylis-Hillman bromides in aqueous media Nature Protocols, 2 (11). pp. 2665-2676. ISSN 1754-2189
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Official URL: http://www.nature.com/nprot/journal/v2/n11/abs/npr...
Related URL: http://dx.doi.org/10.1038/nprot.2007.369
Abstract
This protocol is for an expedient and operationally simple one-pot synthesis of 2-methylenealkanoates and alkanenitriles in high yields from the corresponding Baylis-Hillman bromides. The reaction proceeds via the successive treatment with 1,4-diazabicyclo(2.2.2)octane (DABCO) for 15 min and sodium borohydride for 15 min in aqueous media [tetrahydrofuran (THF):H2O (1:1)] at room temperature.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Nature Publishing Group. |
| ID Code: | 3947 |
| Deposited On: | 13 Oct 2010 07:10 |
| Last Modified: | 13 Oct 2010 07:10 |
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