Bhattacharjee, Manish ; Chaudhuri, Mihir K. (1987) Direct synthesis of ammonium monofluorophosphate monohydrate, [NH4]2[PO3F].H2O and potassium monofluorophosphate, K2[PO3F] Journal of the Chemical Society, Dalton Transactions (2). pp. 477-478. ISSN 0300-9246
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Official URL: http://www.rsc.org/publishing/journals/DT/article....
Related URL: http://dx.doi.org/10.1039/DT9870000477
Abstract
A new direct general method for the synthesis of crystalline [NH4]2[PO3F].H2O and K2[PO3F], based on the reaction of H3PO4 and AHF2(A = NH4 or K) followed by precipitation with ethanol, is described. The identity of the compounds has been established from the results of elemental analyses, molar conductance measurements, i.r. and laser Raman spectroscopic studies. Advantages of the new method are highlighted.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Royal Society of Chemistry. |
| ID Code: | 23521 |
| Deposited On: | 25 Nov 2010 13:12 |
| Last Modified: | 30 May 2011 07:42 |
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