Singh, Satyendra ; Krupanidhi, S. B. (2010) Synthesis and studies of Pb0.76Ca0.24TiO3 nanoparticles derived by sol-gel Advanced Science Letters, 3 (4). pp. 363-367. ISSN 1936-6612
![]()
|
PDF
- Publisher Version
3MB |
Official URL: http://www.ingentaconnect.com/content/asp/asl/2010...
Related URL: http://dx.doi.org/10.1166/asl.2010.1136
Abstract
Pb0.76Ca0.24TiO3 (PCT24) nanoparticles were synthesized by modified sol-gel method and characterized by a number of experimental techniques such as X-ray diffraction, TGA-DTA, FTIR and transmission electron microscopy equipped with energy-dispersive X-ray spectroscopy (EDX). X-ray diffraction (XRD) and selected-area electron diffraction (SAED) investigations demonstrated that the postannealed (650 ° C for 1 h) PCT24 nanoparticles have tetragonal perovskite crystal structure. TEM have been employed to characterize the morphology, structure and composition of the as prepared nanoparticles. Dielectric results indicates the evidence for relaxor type behavior while observed leaky ferroelectric loops may be because of the defects such as grain boundaries and the pores in the sample as the sample was not heated at higher temperature, to retain the nanosize dimension of the particles.
Item Type: | Article |
---|---|
Source: | Copyright of this article belongs to American Scientific Publishers. |
ID Code: | 19258 |
Deposited On: | 23 Nov 2010 13:14 |
Last Modified: | 17 May 2016 03:50 |
Repository Staff Only: item control page