Polshettiwar, Vivek ; Varma, Rajender S. (2007) Tandem bis-aldol reaction of ketones: A facile one-pot synthesis of 1,3-dioxanes in aqueous medium The Journal of Organic Chemistry, 72 (19). pp. 7420-7422. ISSN 0022-3263
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Official URL: https://doi.org/10.1021/jo701337j
Related URL: http://dx.doi.org/10.1021/jo701337j
Abstract
A novel tandem bis-aldol reaction of ketone with paraformaldehyde catalyzed by polystyrenesulfonic acid in aqueous medium delivers 1,3-dioxanes in high yield. This one-pot, operationally simple microwave-assisted synthetic protocol proceeds efficiently in water in the absence of organic solvent, with excellent yield.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to American Chemical Society. |
| ID Code: | 140529 |
| Deposited On: | 24 Dec 2025 09:51 |
| Last Modified: | 24 Dec 2025 09:51 |
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