Hatial, Ishita ; Mukherjee, Raja ; Senapati, Kalyan ; Basak, Amit (2015) Sodium sulfide in methanol: a two-in-one reagent for deprotection of silyl and formation of propargyl sulfide Tetrahedron Letters, 56 (29). pp. 4275-4279. ISSN 0040-4039
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Official URL: http://doi.org/10.1016/J.Tetlet.2015.04.104
Related URL: http://dx.doi.org/10.1016/J.Tetlet.2015.04.104
Abstract
A new reagent Na2S/MeOH for silyl deprotection has been developed. The reagent has several advantages which include deprotection of C-TMS, O-TMS, O-TBS, and O-TBDPS, selective removal of C-TMS and O-TMS in the presence of O-TBS and simultaneous desilylation and sulfide formation in one pot.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Elsevier Science. |
| ID Code: | 130004 |
| Deposited On: | 05 Dec 2022 05:40 |
| Last Modified: | 05 Dec 2022 05:40 |
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