SYNTHESIS AND CHARACTERISATION OF TITANIUM(IV) COMPLEXES OF BENZILMONOTHIOSEMICARBAZONE

Singh, M. S. ; Khan, Shakeela ; Tripathi, U. N. (1997) SYNTHESIS AND CHARACTERISATION OF TITANIUM(IV) COMPLEXES OF BENZILMONOTHIOSEMICARBAZONE Phosphorus, Sulfur, and Silicon and the Related Elements, 130 (1). pp. 107-113. ISSN 1042-6507

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Official URL: http://doi.org/10.1080/10426509708033702

Related URL: http://dx.doi.org/10.1080/10426509708033702

Abstract

Titanium(IV) derivatives of benzilmonothiosemicarbazone have been synthesised by the reaction of titanium tetrachloride with the sodium salt of benzilmonothiosemicarbazone (prepared in situ) in 1: 1, 1:2, 1:3 and 1:4 molar ratios and have been characterised on the basis of elemental (C, H, N, S, C1 and Ti) analyses, molecular weight determinations and spectral (IR and PMR) studies.

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