Singh, M. S. ; Singh, Pratibha ; Gupta, Ashutosh (2010) ChemInform Abstract: Designing Hydroxy-Functionalized Chiral Salen Ligand (III) and Its Use in the Synthesis of Dioxadiazasilamacroheterocycles ChemInform, 41 (47). no-no. ISSN 0931-7597
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Official URL: http://doi.org/10.1002/chin.201047170
Related URL: http://dx.doi.org/10.1002/chin.201047170
Abstract
Synthesis of dioxadiazasilamacroheterocycles is described. The key step involves the initial synthesis of symmetrical hydroxyl-functionalized chiral salen ligand, N, N-bis(2- hy droxy acetophenony lidene)-1, 2-diaminocy clohexane followed by sequential deprotonation with NaH to form dianion intermediate in situ, which reacts with diorganodichlorosilanes to furnish desired heterocycles. The products have been characterized by satisfactory elemental analyses and spectral (IR, 1H 13C, 29Si NMR and mass) studies
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to John Wiley and Sons. |
| ID Code: | 119671 |
| Deposited On: | 16 Jun 2021 06:29 |
| Last Modified: | 16 Jun 2021 06:29 |
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