Nath, Jayashree ; Jamir, Latonglila ; Patel, Bhisma K. (2011) Improved procedure for the preparation of isothiocyanates via iodine-mediated desulfurization of dithiocarbamic acid salts Green Chemistry Letters and Reviews, 4 (1). pp. 1-34. ISSN 1751-8253
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Official URL: https://www.tandfonline.com/doi/abs/10.1080/175182...
Related URL: http://dx.doi.org/10.1080/17518253.2010.486773
Abstract
We report here an improved procedure for the synthesis of isothiocyanates from the corresponding dithiocarbamic acid salts via a desulfurization strategy using molecular iodine and sodium bicarbonate in water/ethyl acetate biphasic medium. The reagents used are easily available, non-toxic, and cheap. High environmental acceptability of the reagents, cost effectiveness and high yields are the important attributes of this methodology.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Taylor & Francis. |
| Keywords: | Iodine; Desulfurization; Oxidation; Isothiocyanate; Sodium Bicarbonate |
| ID Code: | 113921 |
| Deposited On: | 30 Apr 2018 12:26 |
| Last Modified: | 30 Apr 2018 12:26 |
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