Dastidar, P. ; Shankar, V. N. ; Madyastha, K. M. ; Row, T. N. Guru (1992) Structure of 9α,19-dihydroxy-4-androstene-3,17-dione Acta Crystallographica Section C, 48 (3). pp. 486-488. ISSN 0108-2701
|
PDF
- Other
354kB |
Official URL: http://scripts.iucr.org/cgi-bin/paper?S01082701910...
Related URL: http://dx.doi.org/10.1107/S0108270191009319
Abstract
C19H26O4, M1 = 318.41, orthorhombic, P212121, a = 10.591 (1), b = 11.133 (1), c = 13.657 (2) Å, V – 1610.29 Å3, Z = 4, Dm (flotation in KI) = 1.301, Dx = 1.313 g cm-3, Mo Kα, Å = 0.7107 Å, μ = 0.85 cm-1, F(000) = 688, T = 293 K, R – 0.057 for 1253 significant reflections. The Å ring is disordered with atoms C(2) and O(19) occupying two possible sites. The molecules are held together by a hydrogen bond [O(9)…O(17) = 2.89 Å].
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to International Union of Crystallography. |
| ID Code: | 112820 |
| Deposited On: | 19 Apr 2018 11:24 |
| Last Modified: | 19 Apr 2018 11:24 |
Repository Staff Only: item control page
