Bhowmick, K. C. ; Prasad, K. R. K. ; Joshi, N. N. (2002) Synthesis and resolution of 2,2-dimethyl-1,3-diphenyl-1,3-propanediol, a new C2-symmetric and conformationally rigid acyclic diol Tetrahedron: Asymmetry, 13 (8). pp. 851-855. ISSN 0957-4166
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Official URL: http://www.sciencedirect.com/science/article/pii/S...
Related URL: http://dx.doi.org/10.1016/S0957-4166(02)00185-4
Abstract
Diastereomerically pure (+)- and (−)-2,2-dimethyl-1,3-diphenyl-1,3-propanediols were synthesized starting from diethyl malonate and resolved through diesters of (−)-camphanic acid and also N-carbethoxy-l-proline. The absolute configuration of the (−)-enantiomer was established by X-ray crystallography.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Elsevier Science. |
| ID Code: | 106039 |
| Deposited On: | 21 Dec 2017 12:04 |
| Last Modified: | 21 Dec 2017 12:04 |
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