Snyder, John K. ; Zhang, Xiaolin ; Joshi, Balawant S. ; William Pelletier, S. (1989) Complete spectral assignments of tatsidine by two-dimensional NMR techniques Magnetic Resonance in Chemistry, 27 (11). pp. 1057-1064. ISSN 0749-1581
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Official URL: http://onlinelibrary.wiley.com/doi/10.1002/mrc.126...
Related URL: http://dx.doi.org/10.1002/mrc.1260271109
Abstract
Homonuclear 1H COSY, long-range COSY and relay coherence transfer (RCT) correlation spectroscopy NMR experiments were used together with fixed-evolution HETCOR and selective INEPT spectra for complete 13C and 1H spectral peak assignments for tatsidine. Stereochemical and conformational assignments were made from the two-dimensional NOE spectrum. The results of these studies confirmed the location of the methylenedioxy group at C-7/C-8.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to John Wiley and Sons. |
| Keywords: | Long-range COSY; Double Quantum Coherence Correlation Spectroscopy (DQCOSY); Fixed-evolution HETCOR; HOMO 2DJ;2D NOE; Difference Saturation Transfer; Norditerpenoid Alkaloid Selective INEPT; Tatsidine |
| ID Code: | 86880 |
| Deposited On: | 13 Mar 2012 14:57 |
| Last Modified: | 13 Mar 2012 14:57 |
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