A volumetric method for the determination of sulphoxides

Savant, V. V. ; Gopalakrishnan, J. ; Patel, C. C. (1968) A volumetric method for the determination of sulphoxides Fresenius' Journal of Analytical Chemistry, 238 (4). pp. 273-275. ISSN 0937-0633

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Official URL: http://www.springerlink.com/content/l7u2316r373166...

Related URL: http://dx.doi.org/10.1007/BF00499727


A volumetric method for the quantitative determination of Sulphoxides has been developed, based on their oxidation to sulphones by dichromate in presence of 5 M sulphuric acid at 105-110°C. Excess dichromate is titrated by ferrous ammonium sulphate solution. The method is also applicable to the determination of Sulphoxides in metal sulphoxide complexes.

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