Bharadwaj, Parimal K. ; Arbuckle, Brian W. ; Kenneth Musker, W. (1988) Structure of a novel neutral lead(II) complex with dipropyldithiocarbamate Inorganica Chimica Acta, 142 (2). pp. 243-246. ISSN 0020-1693
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Official URL: http://www.sciencedirect.com/science/article/pii/S...
Related URL: http://dx.doi.org/10.1016/S0020-1693(00)81567-4
Abstract
The synthesis and X-ray structure of a novel tetramer of Pb(II) with the dipropyldithiocarbamato ligand is described. The compound crystallizes in the triclinic space group P ̅1with a=9.576(2), b= 14.151(4), c=16.175(4) Å , α =104.84(2), β = 102.26(2), γ =90.62(2)ۥ , V=2065(1) Å 3. Unit cell dimensions and data collection were done at 130(1) K using graphite-monochromated Mo Kα radiation. The conventional R factor is 0.030 for 5323 unique observed reflections with the goodness- of-fit parameter = 1.35. The structure consists of a sulfur-bridged neutral tetrameric species where each Pb(II) ion is pentacoordinated.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Elsevier Science. |
| ID Code: | 78684 |
| Deposited On: | 23 Jan 2012 03:49 |
| Last Modified: | 23 Jan 2012 03:49 |
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