Paul, Ram Chand ; Kumar, R. C. ; Verma, Rajendar Dev (1978) Preparation, characterization and acceptor properties of tris(fluorosulphato)vanadium(III) Journal of Fluorine Chemistry, 11 (3-4). pp. 203-210. ISSN 0022-1139
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Official URL: http://www.sciencedirect.com/science/article/pii/S...
Related URL: http://dx.doi.org/10.1016/S0022-1139(00)82441-0
Abstract
Tris(fluorosulphato)vanadium(III) has been synthesised by interacting vanadium(III) chloride and fluorosulphuric acid. Its complexes with pyridine, ethylenediamine and triphenylphosphine oxide have also been isolated. In all these complexes, the infrared spectra suggest the lower symmetry of fluorosulphate groups and the magnetic moment values are in close proximity for a d2 system. The reflectance spectra reveal the hexacoordination around vanadium(III). Thermal analysis corresponds to four steps decomposition for tris(fluorosulphato)vanadium(III).
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Elsevier Science. |
| ID Code: | 77077 |
| Deposited On: | 09 Jan 2012 14:29 |
| Last Modified: | 09 Jan 2012 14:29 |
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