Application of two-dimensional correlation spectroscopy for assignment of NMR spectra of peptides

Thomas, Albert ; Narasinga Rao, B. N. ; Balaram, P. ; Anil Kumar, (1984) Application of two-dimensional correlation spectroscopy for assignment of NMR spectra of peptides Current Science, 53 (5). pp. 225-230. ISSN 0011-3891

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Abstract

Two-dimensional correlated NMR experiments have been utilized for resonance assignments of two cyclic cystine peptides (I) Boc-Cys-Pro-Leu-Cys-NHMe and (II) Boc-Cys-Gly-Pro-Cys-NHMe and a linear hexapeptide (III) Boc-Asp(Bzl)-Leu-Thr-Gly-Gly-Val-OBzl. Complete resonance assignments have been obtained, by a single two-dimensional correlated experiment in each case. The details of resonance assignment are outlined.

Item Type:Article
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ID Code:72625
Deposited On:29 Nov 2011 09:16
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