Guru Row, Tayur N. ; Venkatesan, Kailasam ; Sharma, Vijay K. ; Kasturi, Tirumalai R. (1975) Crystal and molecular structure of 8a-bromo-1,2,3,5,6,7,8,8a-octahydro-1,3-dioxoisoquinoline-4-carbonitrile Journal of Chemical Society, Perkin Transactions 2, 2 (14). pp. 1597-1600. ISSN 0300-9580
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Official URL: http://pubs.rsc.org/en/Content/ArticleLanding/1975...
Related URL: http://dx.doi.org/10.1039/P29750001597
Abstract
The crystal structure of the title compound has been determined by the heavy-atom method from 1 113 observed three-dimensional photographic data. Crystals are monoclinic with a=17.05, b=7.11, c=17.10 Å(all ±0.02 Å), β=89.0 (0.2)° , space group C2/c, with Z= 8. The structure was refined by block-diagonal least-squares to R 0.098. There is an intermolecular hydrogen bond of the N-H … O type. The cyclohexane portion of the molecule adopts a slightly distorted chair conformation.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Royal Society of Chemistry. |
| ID Code: | 66608 |
| Deposited On: | 27 Oct 2011 04:01 |
| Last Modified: | 16 Jul 2012 08:33 |
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