A new experimental method for heteronuclear correlation spectroscopy with cross-polarization

Chandrakumar, N. ; Nagayama, K. (1987) A new experimental method for heteronuclear correlation spectroscopy with cross-polarization Chemical Physics Letters, 133 (4). pp. 288-292. ISSN 0009-2614

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Official URL: http://dx.doi.org//10.1016/0009-2614(87)87069-0

Related URL: http://dx.doi.org/10.1016/0009-2614(87)87069-0

Abstract

A new experiment is proposed for two-dimensional heteronuclear correlation spectroscopy. It involves the rapid creation of pure heteronuclear ZQC under cross-polarization, followed by an evolution period during which ZQC is converted to DQC. A read pulse is used to detect the signal. No phase cycling is required to determine the sign of ω1

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