Studies on the synthesis of ETS-10 II. Use of organic templates

Das, Tapan Kr. ; Chandwadkar, A. J. ; Budhkar, A. P. ; Sivasanker, S. (1996) Studies on the synthesis of ETS-10 II. Use of organic templates Microporous Materials, 5 (6). pp. 401-410. ISSN 0927-6513

Full text not available from this repository.

Official URL: http://www.sciencedirect.com/science/article/pii/0...

Related URL: http://dx.doi.org/10.1016/0927-6513(95)00075-5

Abstract

ETS-10 has been synthesized using titanosilicate gels and organic templating agents such as choline chloride [OHCH2CH2(CH3)3N+Cl] and the bromide salt of hexaethyl diquat-5 [Br(C2H5)3N+(CH2)5N+(C2H5)3Br]. The influences of temperature and concentration of the ingredients on the kinetics of synthesis are reported. Physicochemical characterizations of the samples have been carried out by X-ray diffraction (XRD), scanning electron microscopy (SEM), infrared (IR) spectroscopy, nuclear magnetic resonance (NMR) spectroscopy and differential thermogravimetric analysis (DTA)/thermogravimetric analysis (TGA), and adsorption of water, n-hexane and mesitylene. The catalytic activities of H-ETS-10 in the dehydration of n-butanol and in the isomerization of m-xylene and 1,3,5-trimethylbenzene are reported.

Item Type:Article
Source:Copyright of this article belongs to Elsevier Science.
Keywords:ETS-10; Titanosilicate; ETS-10; Synthesis Of; ETS-10; Synthesis Using Templates; Choline Chloride; Hexaethyl Diquat-5
ID Code:47675
Deposited On:12 Jul 2011 05:12
Last Modified:12 Jul 2011 05:12

Repository Staff Only: item control page