Structure of p,p'-dinitrobenzanilide

Hariharan , M. ; Srinivasan, R. (1960) Structure of p,p'-dinitrobenzanilide Acta Crystallographica Section C, 46 (6). pp. 1056-1058. ISSN 0108-2701

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C13H9N3O5, Mr=287.2, monoclinic, P21/n, a=6.230(1), b=17.922(4), c=11.562(2)Å, β=105.50(1)°, V=1244.0(4)Å3, Z=4, Dm=1.53(2), Dx=1.537gcm-3, λ(CuKα)=1.5418Å, μ=9.24cm-1, T=293K, F(000)=592, R=0.062, wR=0.064 for 1004 reflections with I≥3σ(I). The amide plane makes an angle of 16.4(4) and 17.5(4)° respectively with the two benzene rings. The benzene rings are at 3.0(1)° with respect to each other.

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