Growth of single crystals of KClO4 in silica gels

Patel, Ambalal Ranchhodhbhai ; Rao, A. Venkateswara (1977) Growth of single crystals of KClO4 in silica gels Journal of Crystal Growth, 38 (3). pp. 288-292. ISSN 0022-0248

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Official URL: http://linkinghub.elsevier.com/retrieve/pii/002202...

Related URL: http://dx.doi.org/10.1016/0022-0248(77)90348-7

Abstract

Single crystals of KClO4 up to 20×10×6 mm size have been grown in silica gels at ambient temperature and identified by X-ray diffraction and suitable chemical analysis. The crystals are grown with different crystallization apparatus, different reactants and the effect of reaction waste products on crystal quality and size has been studied. The effect of concentration of reactants on habit modification has also been studied. It is observed the at lower concentration of reactants, crystals with large {101}, {210} and smaller {001} habit faces grow, while at higher concentrations, {001} faces disappear and the crystal grow in the form of needles. Cups have been observed during the growth of these crystals.

Item Type:Article
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ID Code:32816
Deposited On:03 May 2011 13:53
Last Modified:03 May 2011 13:53

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