Clark, H. C. ; Jain, V. K. ; McMahon, I. J. ; Mehrotra, R. C. (1983) The stereochemistry of organotin(IV) oxinates in solution: TIN-119 nuclear magnetic resonance study of triorganotin(IV) oxinates Journal of Organometallic Chemistry, 243 (3). pp. 299-303. ISSN 0022-328X
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Official URL: http://dx.doi.org/10.1016/S0022-328X(00)98551-6
Related URL: http://dx.doi.org/10.1016/S0022-328X(00)98551-6
Abstract
Contrary to the previously proposed fluxional trigonal bipyramidal structure for triorganotin(IV) oxinates, the 119Sn NMR chemical shifts of these compounds are consistent with tetrahedral, 4 coordinate tin. No fluxional processes could be detected in the 1H and 13C NMR spectra of Me3SnOx down to -90°C.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Elsevier Science. |
| ID Code: | 30186 |
| Deposited On: | 22 Dec 2010 10:44 |
| Last Modified: | 07 Jun 2011 06:17 |
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