Synthesis and X-ray crystal structure of 1,3,5-tris(fluoren-9-ylidenemethyl)benzene: towards a C48-fragment of [60]-fullerene

Mehta, Goverdhan ; Venkateswara Rao, K. ; Ravikumar, K. (1995) Synthesis and X-ray crystal structure of 1,3,5-tris(fluoren-9-ylidenemethyl)benzene: towards a C48-fragment of [60]-fullerene Journal of the Chemical Society, Perkin Transactions 1 (14). pp. 1787-1788. ISSN 0300-922X

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Official URL: http://pubs.rsc.org/en/Content/ArticleLanding/1995...

Related URL: http://dx.doi.org/10.1039/P19950001787

Abstract

Three-fold, stereoselective Wittig reactions between benzene-1, 3, 5-tricarbaldehyde 4 and fluoren-9-ylidene(triphenyl)phosphine 5 furnished an interesting C48-hydrocarbon of C3symmetry whose crystal structure has been determined.

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