Natarajan, Srinivasan ; Cheetham, Anthony K. (1998) Synthesis and structural characterization of a layered tin (II) phosphate,[Sn2(PO4)2]2-[C2 N2H10]2+·H2O Journal of Solid State Chemistry, 140 (2). pp. 435-439. ISSN 0022-4596
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Official URL: http://linkinghub.elsevier.com/retrieve/pii/S00224...
Related URL: http://dx.doi.org/10.1006/jssc.1998.7878
Abstract
A new layered tin(II) phosphate [Sn2(PO4)2]2- [C2N2H10]2+·H2O was synthesized by hydrothermal technique. It crystallizes in monoclinic space group P21/c (No. 14) with lattice parameters a=9.4112(1) Å; b=8.5998(1) Å; c=15.9921(2) Å; β=100.009(1)°; V=1274.61(2);Z=4; R=2.06%; Rw=2.17%. The structure consists of inorganic layers, comprising a network of strictly alternating SnO3 and PO4 moieties and held together by strong hydrogen bonding between the layers. Protonated ethylenediamine and water molecules are trapped between the layers.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Elsevier Science. |
| ID Code: | 27688 |
| Deposited On: | 11 Dec 2010 08:26 |
| Last Modified: | 11 Dec 2010 08:26 |
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