Synthesis of (3R,4S,5S,9S)-3,5,9-trihydroxy-4-methylundecanoic acid δ-lactone

Chakraborty, Tushar K. ; Goswami, Rajib K. (2004) Synthesis of (3R,4S,5S,9S)-3,5,9-trihydroxy-4-methylundecanoic acid δ-lactone Tetrahedron Letters, 45 (41). pp. 7637-7639. ISSN 0040-4039

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Radical-mediated opening of a chiral trisubstituted epoxy alcohol using cp2TiCl furnished the '2-methyl-1,3-diol' moiety with the desired stereochemistry, which led to a total synthesis of (3R,4S,5S,9S)-3,5,9-trihydroxy-4-methylundecanoic acid δ-lactone 1.

Item Type:Article
Source:Copyright of this article belongs to Elsevier Science.
Keywords:(3R,4S,5S,9S)-3; 5; 9-Trihydroxy-4-methylundecanoic Acid; δ-Lactone; Sharpless Kinetic Resolution; Epoxide Opening; 2-Methyl-1; 3-diol
ID Code:20563
Deposited On:20 Nov 2010 14:18
Last Modified:22 May 2011 15:04

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