Rajagopalan, T. G. ; Anjaneyulu, B. ; Shanbag, V. D. ; Grewal, R. S. (1981) Electron-capture gas chromatographic assay for primaquine in blood Journal of Chromatography B: Biomedical Sciences and Applications, 224 (2). pp. 265-273. ISSN 0378-4347
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Official URL: http://linkinghub.elsevier.com/retrieve/pii/S03784...
Related URL: http://dx.doi.org/10.1016/S0378-4347(00)80164-4
Abstract
A sensitive gas chromatographic method for the quantitative determination of the anti-malarial drug primaquine is described. The method involves derivatization with heptafluorobutyric anhydride to form the diheptafluorobutyramide derivative after a single extraction at alkaline pH. The derivatives are quantitated by electron-capture gas chromatography. Blood levels of primaquine as low as 8 ng/ml can be measured with good precision.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Elsevier Science. |
| ID Code: | 15534 |
| Deposited On: | 13 Nov 2010 09:21 |
| Last Modified: | 02 Jun 2011 06:06 |
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