Yadav, K. Mallik ; Suresh, Joghee R. ; Patro, Balaram ; Ila, Hiriyakkanavar ; Junjappa, Hiriyakkanavar (1996) Stepwise controlled reduction of α-oxoketene dithioacetals with Zn/ZnCl2-TMEDA in ethanol Tetrahedron, 52 (13). pp. 4679-4686. ISSN 0040-4020
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Official URL: http://linkinghub.elsevier.com/retrieve/pii/004040...
Related URL: http://dx.doi.org/10.1016/0040-4020(96)00139-1
Abstract
α-Oxoketene dithioacetals 1 are shown to undergo highly selective conjugate reduction with Zn/ZnCl2-TMEDA in refluxing ethanol under controlled reaction conditions to afford β-methylthiomethylene ketones 6, β-methylthioketones 7 and the completely desulphurized α-methylketones 8 in sequential manner.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Elsevier Science. |
| ID Code: | 15324 |
| Deposited On: | 13 Nov 2010 12:56 |
| Last Modified: | 22 Feb 2011 08:25 |
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