Sabitha, Gowravaram ; Gurumurthy, Chevula ; Yadav, Jhillu (2014) The First Total Synthesis of Pectinolide F Synthesis, 46 (13). pp. 1757-1764. ISSN 0039-7881
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Official URL: http://doi.org/10.1055/S-0033-1341231
Related URL: http://dx.doi.org/10.1055/S-0033-1341231
Abstract
The first total synthesis of the natural saturated α-pyrone pectinolide F has been accomplished from inexpensive, commercially available (S)-ethyl lactate and but-3-yn-1-ol. The salient features of the synthesis are 2,2,6,6-tetramethylpiperidin-1-oxyl (TEMPO)–[bis(acetoxy)iodo]benzene oxidation, Sharpless asymmetric dihydroxylation, Grignard reaction, and partial hydrogenation of the triple bond.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Georg Thieme Verlag KG. |
| ID Code: | 135660 |
| Deposited On: | 17 Jul 2023 07:57 |
| Last Modified: | 17 Jul 2023 07:57 |
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