Combined Cryo and Room-Temperature Ball Milling to Produce Ultrafine Halide Crystallites

Verma, Akash ; Biswas, Krishanu ; Tiwary, Chandra Sekhar ; Mondal, Amit Kumar ; Chattopadhyay, Kamanio (2011) Combined Cryo and Room-Temperature Ball Milling to Produce Ultrafine Halide Crystallites Metallurgical and Materials Transactions A, 42 (4). pp. 1127-1137. ISSN 1073-5623

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Official URL: http://doi.org/10.1007/s11661-010-0490-1

Related URL: http://dx.doi.org/10.1007/s11661-010-0490-1

Abstract

The combined milling at cryogenic temperature as well as room temperature (RT) has been carried out to prepare ultrafine NaCl crystallites. The milling has been done in evacuated tungsten carbide vials backfilled with high-purity Ar. The results indicate the effect duration of cryomilling prior to RT milling has a strong effect on the final crystallite size. The deformation aided sintering of NaCl crystallites during RT milling and leads to the formation of bimodal distribution of crystallites. The cuboidal-shaped NaCl crystallite undergoes a roughening transition due to plastic deformation. The experimental results are explained using the temperature-dependent mechanical properties of NaCl single crystals and plastic-deformation-induced roughening.

Item Type:Article
Source:Copyright of this article belongs to Springer Nature Switzerland AG
Keywords:Milling;Shear Band;Mechanical Milling;Resistance Temperature Detector;High Magnification Micrograph
ID Code:135372
Deposited On:23 Jan 2023 04:50
Last Modified:23 Jan 2023 04:50

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