A rapid method for the synthesis of nitrogen doped TiO2 nanoparticles for photocatalytic hydrogen generation

Jayakumar, Onattu Damodaran ; Sasikala, Rajamma ; Betty, Chirayath Antony ; Tyagi, Avesh Kumar ; Bharadwaj, Shyamala Rajkumar ; Gautam, Ujjal Kumar ; Srinivasu, Pavuluri ; Vinu, Ajayan (2009) A rapid method for the synthesis of nitrogen doped TiO2 nanoparticles for photocatalytic hydrogen generation Journal of Nanoscience and Nanotechnology, 9 (8). pp. 4663-4667. ISSN 1533-4880

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Official URL: http://www.ingentaconnect.com/content/asp/jnn/2009...

Related URL: http://dx.doi.org/10.1166/jnn.2009.1273

Abstract

A facile, fast, and economic method of doping TiO2, synthesized by conventional precipitation route with N has been developed. By this method, stable N doped TiO2 can be prepared within a short duration of time. The method adopted was to treat the TiO2 powder synthesized by simple precipitation with trioctyl amine (TOA) at 320 °C for 2 hours followed by calcination at 400 °C for 2 hours to obtain the N-doped TiO2. The sample along with NiO as co-catalyst showed significant photocatalytic activity for hydrogen generation from aqueous methanol solution under sunlight type irradiation. This synthesis method opens up a fast and easy route for doping the existing TiO2 or other wide band gap oxide semiconductors with nitrogen so that they can exhibit enhanced photocatalytic activity under solar irradiation.

Item Type:Article
Source:Copyright of this article belongs to American Scientific Publishers.
Keywords:Hydrogen Generation; N Doped TiO2; Nanoparticles; Photocatalyst; Sun Light Type Radiation
ID Code:108127
Deposited On:01 Feb 2018 11:31
Last Modified:01 Feb 2018 11:31

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