Prasad, Kavirayani ; Sunnam, Sunil (2013) Total synthesis of (+)-pinellic acid Synthesis, 45 (14). pp. 1991-1996. ISSN 0039-7881
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Official URL: https://www.thieme-connect.com/products/ejournals/...
Related URL: http://dx.doi.org/10.1055/s-0033-1338799
Abstract
A straightforward strategy for the synthesis of (+)-pinellic acid in 16% overall yield and 13 steps, starting from (1R)-1-(furan-2-yl)hexan-1-ol, is described. Key reactions in the synthesis include a Sharpless kinetic resolution, oxidation of a protected furan to reveal a but-2-ene-1,4-dione moiety, and an asymmetric reduction.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Thieme Medical Publishers Inc. |
| Keywords: | Pinellic Acid; Furan Oxidation; Natural Products; Total Synthesis |
| ID Code: | 105634 |
| Deposited On: | 21 Dec 2017 12:05 |
| Last Modified: | 21 Dec 2017 12:05 |
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