Clark, J. N. ; Jagannathan, N. R. ; Herring, F. G. (1989) High-resolution solid-state exp 13 C CP/MAS nuclear magnetic resonance study of poly(p-phenylene sulphide) Polymer Communications, 30 (7). pp. 212-214. ISSN 0263-6476
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Abstract
The solid-state exp 13 C n.m.r. spectrum of poly(p-phenylene sulphide) (PPS) was obtained using cross-polarization (CP) and magic angle spinning (MAS) techniques. The two magnetically distinct carbon atoms were easily assigned using an interrupted decoupling experiment. PPS samples of varying degrees of crystallinity were prepared above and below the glass transition temperature T sub g and the corresponding exp 13C CP/MAS n.m.r. spectra were obtained. The line-width of the exp 13 C spectra was found to be a function of crystallinity.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Butterworth. |
| Keywords: | Polyphenylene Sulfides ; Atomic Properties ; Nuclear Magnetic Resonance ; Crystal Structure ; Line Spectra ; Microstructural Effects |
| ID Code: | 74300 |
| Deposited On: | 12 Dec 2011 04:13 |
| Last Modified: | 12 Dec 2011 04:13 |
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