Bhuniya, Debnath ; Singh, Vinod K. (1994) Enantioselective deprotonation of cyclohexene oxide to (R)-2-cyclohexen-1-ol Synthetic Communications, 24 (10). pp. 1475-1481. ISSN 0039-7911
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Official URL: http://www.tandfonline.com/doi/abs/10.1080/0039791...
Related URL: http://dx.doi.org/10.1080/00397919408011752
Abstract
The reaction of cyclohexene oxide with homochiral lithium amides, prepared from (S)-phenylglycine and (S)-valine has been studied and (R)-2-cyclohexen-1-ol 3 was prepared in a maximum of 72% ee. The optical purity was determined by 1H NMR measurement of the α-methoxy-α-(trifluoromethyl)phenyl acetic acid (MTPA) derivative of the corresponding alcohol.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Taylor and Francis Group. |
| ID Code: | 55166 |
| Deposited On: | 18 Aug 2011 08:25 |
| Last Modified: | 18 Aug 2011 08:25 |
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