Datta, A. ; Bhattacharjee, S. ; Ila, H. ; Junjappa, H. (1988) Polarized ketene dithioacetals; 71.1 Synthesis of 2,5-substituted 3-bis(methylthio)methylenetetrahydrofurans Synthesis, 1988 (9). pp. 725-727. ISSN 0039-7881
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Official URL: https://www.thieme-connect.com/ejournals/abstract/...
Related URL: http://dx.doi.org/10.1055/s-1988-27689
Abstract
Synthesis of novel 2,5-substituted 3-bis(methylthio)methylenetetrahydrofurans 4 by oxymercuration-reduction of α- bis(methylthio) methylene-γ,δ-unsaturated alcohols 2 is reported. The carbinols 2 are obtained from the corresponding allyl-(or 2-methyl-2-propenyl) acylketene dithioacetals 1 by sodium borohydride reduction or by treatment with methylmagnesium iodide.
| Item Type: | Article |
|---|---|
| Source: | Copyright of this article belongs to Thieme Medical Publishers Inc. |
| ID Code: | 15502 |
| Deposited On: | 13 Nov 2010 09:06 |
| Last Modified: | 03 Jun 2011 06:23 |
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